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Dushyant Patel Review of Literature

S.K.P.C.P.E.R., Kherva 8 M .Pharm. Thesis

CHAPTER 2: REVIEW OF LITERATURE

2.1 REVIEW OF LITERATURE:

TABLE NO: 2.1 OFFICIAL ANALYTICAL METHOD

TITLE METHOD EXPERIMENTAL CONDITION

1. USP official Method

HPLC Column: 4.6 mm×25 cm with L1 packing

MP: ACN: phosphate buffer

(24:76, v/v) (pH:1.8)

Detection method: UV detection (215 nm)

Flow rate: 1ml/min

TABLE NO: 2.2 REPORTED ANALYTICAL METHODS

TITLE METHOD EXPERIMENTAL

CONDITION

1. Rapid quantification of gabapentin

in human plasma by LC- MS/MS

LC-MS/MS Column: Waters symmetry

C18 RP

MP: ACN: 10 mM Amm.

formate (80:20, v/v, pH:3.0)

IS: 1,1-Cyclohexane diacetic

acid monoamide

MS mode: MRM

2. Determination of gabapentin in

human plasma using hydrophilic

interaction LC- MS/MS

LC-MS/MS Column: Atlantis HILIC silica

MP: ACN: 100 mM Amm.

formate (85:15, v/v) (pH:3.0)

IS: Metformin

MS mode: MRM

3. Validated LC-MS/MS method for

quantification of gabapentin in

human plasma: application to

pharmacokinetic and BE studies in

Korean volunteers

LC-MS/MS

Column: Gemini C18

MP: ACN: 10 mM Amm.

acetate (20:80, v/v, pH:3.2)

IS: (S)-(+)-alpha-amino

cyclohexanepropionic acid

hydrate

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