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Dushyant Patel LC-MS/MS Method

S.K.P.C.P.E.R., Kherva 56 M .Pharm. Thesis

TABLE NO: 4.16

BETWEEN-BATCH OR INTER-BATCH ACCURACY AND PRECISION OF GBP

Sr.

No.

Day

LLOQ (0.05 µg/ml) LQC (0.15 µg/ml)

Calculated conc. % Nominal conc. Calculated conc. % Nominal conc.

Day 1

0.049 98.00 0.163 108.7

2 0.040 80.00 0.166 110.7

3 0.049 98.00 0.154 102.7

4 0.047 94.00 0.162 108.0

5 0.050 100.0 0.148 98.67

6 0.054 108.0 0.152 101.3

Day 2

0.054 108.0 0.152 101.3

8 0.049 98.00 0.148 98.67

9 0.053 106.0 0.158 105.3

10 0.049 98.00 0.154 102.7

11 0.046 92.00 0.158 105.3

12 0.051 102.0 0.156 104.0

Day 3

0.063 126.0 0.146 97.33

14 0.052 104.0 0.151 100.7

15 0.049 98.00 0.155 103.3

16 0.051 102.0 0.154 102.7

17 0.044 88.00 0.149 99.33

18 0.050 100.0 0.156 104.0

Day 4

0.049 98.00 0.147 98.00

20 0.049 98.00 0.149 99.33

21 0.049 98.00 0.149 99.33

22 0.047 94.00 0.145 96.67

23 0.048 96.00 0.151 100.7

24 0.045 90.00 0.146 97.33

Day 5

0.052 104.0 0.147 98.00

26 0.050 100.0 0.150 100.0

27 0.052 104.0 0.153 102.0

28 0.046 92.00 0.153 102.0

29 0.048 96.00 0.153 102.0

30 0.050 100.0 0.152 101.3

n 30 30

Mean 0.050 99.00 0.153 101.7

SD 0.004

0.005

%CV 7.90 3.38

1 2 ... 63 64 65 66 67 68 69 70 71 72 73 ... 92 93

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Samsung RT34M Manuale Utente Pagina 68

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