Samsung RT34M Manuale Utente Scaricare il pdf (Pagina 21)

Dushyant Patel Review of Literature

S.K.P.C.P.E.R., Kherva 9 M .Pharm. Thesis

4. Gabapentin quantification in human

plasma by high-performance liquid

chromatography coupled to

electrospray tandem mass

spectrometry. Application to

bioequivalence study

5

.

LC-MS/MS Extraction method: Protein

precipitation

Column: C4 RP

MS mode: MRM

5. Quantitative determination of

vigabatrin and gabapentin in human

serum by gas chromatography -

mass spectrometry

6

.

GC-MS

Column: polydimethylsiloxane

IS: Cyclobarbital

MS mode: SIM

6. Analysis of gabapentin in serum

and plasma by solid-phase

extraction and GC-MS for

therapeutic drug monitoring

7

.

GC-MS Extraction method: SPE

Derivatization reagent :

MTBSTFA

7. Determination of gabapentin in

pharmaceutical preparations by

HPTLC

8

.

HPTLC Plate: Aluminum-backed silica

gel 60 F

254

HPTLC plates

MP: n-butanol: water :glacial

acetic acid ( 3:3:2, v/v )

IS: Histamine hydrochloride

8. Development and application of a

validated HPLC method for the

determination of gabapentin and its

major degradation impurity in drug

products

9

.

HPLC Column: Brownlee spheri-5

cyano

MP: ACN:10 mM KH

2

PO

4

/10

mM K

2

HPO

4

(pH 6.2,8:92 v/v)

Detection method: UV

detection at 210 nm

9. A HPLC micro method for the

simultaneous determination of

vigabatrin and gabapentin in

serum

10

.

HPLC

Column:125 x 3-mm ID

Hypersil BDS C-18 column,

3-µ mini-bore

MP : phosphate buffer

(pH 6.5):ACN:methanol:water

1 2 ... 16 17 18 19 20 21 22 23 24 25 26 ... 92 93

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